| Author |
Topic: Meth synth shortcut? |
bluenote Junior
Member |
posted 10-28-1999 03:14 AM
Theoretically, what would be the result of filtering the hi/p/e rxn
diluted with dh20, and utilizing the un-eveporated remains? The reason I
ask is, my grandma has tried to complete the proccess and has major
problems with phing and moving the solution to and from polar/non-polar
solvents. It goes something like this:
After reacting 5g i2, 4g E, and 3g rp............expected signs occur,
ie. yellow/white fumes, bubbling, then thinning maroon mud, ect. add equal
amount dh20, filter several times(reddish color doesnt go away), add
ronsonal, then lye until ph on water is about 12-14. At this point grandma
assumes the goods went into the fuel. Then the water/lye is removed and
replaced with clean water and HCL is added, but ph seems to remain low
despite the amount of HCL added. When water is evaped some wierd crap
remains. Bitter, yet seemingly not ephed or anything else good.
Anyway, the big question is: would it be possible to avoid the proccess
after the main reaction at all? Grandma isnt too concerened with quality
at this point. And is fully aware of how stupid and unskilled she seems,
but shes tried this several times and is sick of baking fucked up cookies!
Thanks for the advice, and flames are more than welcome.
|
CHEMMAN Member |
posted 10-28-1999 06:25 AM
Not concerned with quality??????Leave out the AB extraction??????????
This is so fucking stupid.Why not just swallow some cyanide and
get it over with quicker .Tell Grandma to stick with baking
cookies.
|
spitball Administrator |
posted 10-28-1999 07:24 AM
Shortcut...? Yeah. buy it from someone else.
I hate people sometimes.
-Spitball-
|
Midnight
Rush Member |
posted 10-28-1999 07:47 AM
Tell ya what. After my first dream I'll sell you 3grms for 20 bucks. Well
ok, 250mg cut with the closest powder to me at the time. Atleast your
chances of survival would improve.
|
CHEMMAN Member |
posted 10-28-1999 07:57 AM
If you cant do an AB extraction,you should not do any of this ,let alone
try to shortcut ( it wont work )and possibly harm someone through your
incompetence.Dont close it yet Spitball,they deserve all the shit
coming!!
|
Hematite Member |
posted 10-28-1999 09:22 AM
Actually, now that the topic of shortcuts has been opened.... With all
this pill modification lately in the attempt to thwart our most valiant
efforts and make our lives all work and no play; I now wonder if we
wouldn't have more luck with a little shortcut I've been pondering, and
that is to put any number of untouched pills (of any description-different
effects would be part of the lucky dip)into a blender and then use
worlocks dry and chiled reactants method, except that in this variation we
just use the strongest and acid like stuff we have around. Blend on high
for 3 minutes and carefully filter to remove possible toxic
ingredients(well the bigger bits anyway)and suger to taste and you have a
smoothie that's bound to do something ! Please dont flame just cause
the finer points have been glossed over, and only knowlegable people reply
please
------------------ Regards,Hematite.
|
Xaja Member |
posted 10-28-1999 04:31 PM
Hematite I tried a short-cut much like that once. Took days for my sight
to return...
|
bluenote Junior
Member |
posted 10-28-1999 05:00 PM
CHEMMAN, Spitball:
I guess the "acedemic" aspect of this procedure is the real purpose
here huh? I`m sure "legetimate" chemists really respect your benevolent,
richeous approach to making fucking crank in your garage.
I just wanted to get a simplified A/B method, as my sense of self worth
isnt based on how competant I am at cooking up drugs.
And as per your advice, I injected grandma with 5g of pure cyonide in
her sleep. I`m sure it was a great high, because she twitched and shivered
and foamed at the mouth until peacefully bloating in a pool of her own
excretions.
If were as stupid as you treat me, I guess you wouldnt
feel any sense of guilt for suggesting such a thing if I were to actually
do it. Selective evolution?
Thanks for the help.
|
Sun_Rah Member |
posted 10-28-1999 05:07 PM
I always wondered what it would be like to watch someone do a RP/I2/E
reduction with enough regiments to actually leave the E in all the
fillers, I mean not even extracting it just powder then mix fully,
completely with rp then add I2mix and add a dab of dh20......any one else
thought of this or am i just a dumass with dreams of easiness I am sure I am not
the only one thinking of this? Seems like the oil would still make it
out? Just some thoughts.....
|
Hematite Member |
posted 10-28-1999 06:35 PM
Now see in my shortcut, I would crush a few aspirin, couple of panadol and
a few that the names have rubbed off but really mellow you out....and
hopefully the poison properties of the final product wouldn't hurt too
bad, smart huh !
------------------ Regards,Hematite.
|
Snotbrain Member |
posted 10-28-1999 07:54 PM
If in waren't fer all the stuk-up peeples whut wanna smoke this shee-it,
it woodn't evun mattter if the guauifenereeesding and
gloygenpolycolglugogen and udder stuff were in the produckt.
JUst swaller the stuff and dont to worrry aboot it .
But then, hell, jus take a cuuple uh effedrine and soodyefedrine and
cafienne pills and safe de trubble anyhoo.
snodder
|
Fitzhugh Member |
posted 10-28-1999 10:09 PM
bluenote:
You were not very descriptive of your reduction method or your A/B
extraction method. You could have problems with either.
Based on what I have read elsewhere, after you have raised the pH to
around 12, you need to shake the ronsonal and the water layers together
very thourghly. (In a closed bottle you should shake vigorusly for at
least 2 minutes, venting the bottle every 30 seconds or so.)
After shaking, you need to check the pH of the water layer again to
make sure it is still about 12. If not, add more lye and shake again.
Repeat until the final pH stays near 12.
You will then want to draw off the ronsonol and repeat the process with
one or two more volumes of ronsonol, adding all of the batches of ronsonol
together.
Base on your description of the water extraction, you would then add
water and HCl, once again shaking and checking that the pH remains under 2
or 3, adding more HCl as necessary and shaking more.
Draw off the water layer and repeat the water and HCl steps twice more.
Add all the water volumes together and evaporate the water.
From what I have read, the mixing and checking of the pH are critical
to getting the final product where you want it.
Also from what I have read, there are several places where you could do
some fairly simple cleanup steps that wouldn't reduce you yield, but would
make your product kinder to your bod, and a good deal tastier. I would
recomend you do a bit more reading on purification steps.
|
Midnight
Rush Member |
posted 10-29-1999 01:37 AM
Just a quick correction on your acid phase of the A/B. Ph 3 is way to low.
It should be around ph 7
|
Worlock Member |
posted 10-29-1999 03:09 AM
You want to evaporate away a solution of HI, I2, Meth-I salts, various
ammoniated hydrocarbons and several N,N-biphenyl-ethyl substances
? Might be a little tough to breathe when the HI starts coming off.
The neutralization of the acids, must be done. So why not just raise
the pH to 12 leaving you with meth freebase in a nonpolar solvent. 95%
cleaned by just adding and flushing the lye Then How hard is it to
add water and HCl, shake and reduce the pH to neutral 7.0 to
8.0.
|
bluenote Junior
Member |
posted 10-29-1999 04:07 AM
"How hard is it to add water and HCl, shake and reduce the pH to neutral
7.0 to 8.0."
Well put Worlock. I wondered this myself everytime. I think the problem
has been adding the HCL. The amounts of e/rp/i are so low, when adding
just one drop of HCL seems to put the Ph at a level of below 6. Maybe use
a higher volume of dh20 at this step?
Hmmm, I honestly have no problems with any other stage of this very
simple experiment.
Thanks for the input....
|
Midnight
Rush Member |
posted 10-29-1999 06:38 AM
Or just use a dilute HCL. If you're using hardware store stuff it's
normaly only *trying to remember* like 48% or was it 58% concentration. If
that's to strong mix in a little water. Second thought Would it be
possible to premix a solution to the proper ph and then add it to the
substance? In my uneducated mind it seems that it would work other than
the product giving the premixed solution a base. But that would be easy to
fix by having the ph of the water a little more acid, maybe 6.5 and if the
ph were still a little low you could add a little of the freebase that was
set aside? If it worked would it also have a positive influence on yield
by not having the HCL burning anything before it gets mixed?
Midnight, looking for ways to keep product out of PHing as much as
possible.
|
whoops Member |
posted 10-29-1999 05:02 PM
Try thinking tube furnace the ph varies from top to bottom all ya got to
do is slowly circulate the solution and then let your screen filter out
the goodies in the appropiate dimensional portal, really could not be
simpler
|
cactus Member |
posted 10-29-1999 05:29 PM
This method can work but you should at least strain the I2 water then add
some boiling water to flask to clean that out and then the hot water added
to the I2 reaction solution will be more pleased to release the product
into the uper layer of naptha. Then you will have to remove the naptha
layer and then gas with HCI. Then you will have Methamphetamine crystals
floating around.
Strain this and wash with acitone but you will have to do several pulls
of the I2 water.
Simply add more fuel and sprinkle lye. Even the first time you only
want to sprinkle a little lye. This way you don't burn every thing up at
once. And also if the solvent isn't very dry the HCI gas will not produce
crystals. Then the fuel needs to have a little acetone added and a little
microwave reduction. Simply place into the microwave for 3 minutes as long
as you dont evaperate every thing.
The first pull may be small but second will be large and the 3rd 4th
and 5th will decrease.
You are really doing an A/B extraction. At least It sounds like you are
attempting a harmless proceedure. There are problems with lye but you
should filter each solvent pull and the lye will simply stick to the glass
you need a lot of mason jars and simply decant off fuel untill no lye is
present and then reduce and gas. This is the fastest way to sample you
product 10 minutes after the reaction.
------------------ Live With Freedom
|
Worlock Member |
posted 10-30-1999 01:53 PM
bluenote I am totally lost here. Granny reacted the
I/E/RP, filtered out the RP added ronson fuel, added lye water
to incease pH to 12 -14 shake flush the lye water, I2, I-, and
other trash added fresh water shake add HCl adjust pH to 7-8
quote:
until ph on water is about 12-14 ..... replaced with clean water and HCL
is added, but ph seems to remain low despite the amount of HCL added.
The pH should drop from 12 to 7 How does it "remain"
low??
|
bluenote Junior
Member |
posted 10-30-1999 06:48 PM
Lets see, I think I wrote that backwards. After removing lye/shit
solution, fresh h20 is added. At that point ph is higher than 7-8. So one
drop of hcl is added. That one drop has proved to be too much. It
immediatly lowers ph to 3-4. So, as in my previous post, it was realized
that a greater volume of h20 to add the acid to would be better, as it
would dilute the acid.
Q: If a Ph of 7.5 or so, is not maintained in the water, would that
mean the meth is not released from the fuel? Or just that the meth isnt
functional at any other Ph level?
|
Android Member |
posted 10-30-1999 07:28 PM
You lost Worlock and now you have to go find him! These dedicated soldiers
have sacrificed years out of their lives simplifying this hardware store,
OTC method, and you got it so complicated ya set em back 5 years! Right
on, killer! You rock!
Now, go find Worlock!
------------------ These Irish eyes are smiling!
|
bennie Member |
posted 10-30-1999 11:48 PM
Cactus Could you please elaborate on the microwave/ solvent drying
technique you mentioned Thanks
|
Sawman Member |
posted 10-31-1999 08:27 AM
Listening to these newbees is really funny. Trying to redesine the wheel
again?
|
Hematite Member |
posted 10-31-1999 08:47 AM
After only a brief read, forgive me if this isn't relevant; If one drop
of acid lowers your aqueous solution to 3/4 after thoroughly mixing with
the solvent and having been allowed time to settle before testing....Then
rest assured you have no meth there at all.Sorry.
------------------ Regards,Hematite.
|
Android Member |
posted 10-31-1999 09:43 AM
And we have a winner, folks! Step right up and pick your prize!
------------------ These Irish eyes are smiling!
|
CHEMMAN Member |
posted 11-01-1999 05:45 AM
I am not flaming you now bluenote.Instead I offer a valid shortcut
with purity ,and ease of use.Its called a HCl gas generator . Advantages
are clean product , Quick,No Phing worries.Simply gas np layer.Study
this one up
|
rev
drone Member |
posted 11-01-1999 08:02 AM
I've been working on this for you for a while. I was going to call it the
"twist/lift/twitch" method, then the "yank/turn" method, but I streamlined
the whole process, and came up with the amazing
"shimmy/jolt/push-up-daisies/pull" method. Here's a shortcut:
1. See how much iodine you can dissolve in half a shotglass of
everclear.
2. Add a gram or two of red phosphorous, and a few grams of ephedrine.
3. Over the teeth, and past the gums, look out internal organs, cuz
here it comes! Chug that shot like a real man/woman!! Clearly, your goal
is slowly poisoning yourself, rather than making methaphetamine of decent
quality; so why dilly-dally? This method will certainly accomplish what
you're settig out on, and in a fraction of the time.
------------------ -the good reverend drone
|
whoops Member |
posted 11-01-1999 12:12 PM
Allrighty then lets review this setup!
A it is a tube furnace. b it proc3ess the meterial c it is not
complicated though fine adjustments may be necessary D the reduction
happens because of proposed hypothesis++++++++++++==========the formation
of CO at one of the ellectrodes and precipation until saturation of Naoh
and the reduction because of formation of Co2 co2 is a gas when forming
from CO carbon monoxide this is a reduction this is optomized with solvent
portion to simply steal the available oxygen and leave the ephedrine in
the Clorinated state, cloring to sat on one side of upside down water
glass trick, solvent water could be seperated by upside test tube in
upside down water glass,.....thus we also add a stirrer and this seperates
by graviety the heaveyst up against the wall, um the is a shure way to
figure if this is producing co2? Co? of hydrogen?????
What happens when you mix Naoh Clorine Hcl NaCL hydrogen carbon e- and
water????
The water is reduced to oh the clorine ion is seperated from nacl to
cl2 the hydrogen ion is liberated "" to h+h=H2[g] thus incompatable
in water Na becomes Naoh at the reduction site of the water
Carbon could be considered the metaloid, it is transfered from the
donating electrode to the recieving ellectrode, now who is it in here
thats got that unknown ellement figured out therew was two of them
ellements mentioned I whant details man??????
Ok so ya mix Naoh and Acid, now the big difference between Naoh and
baking soda is what, comon I need this information!!!!
Repeate what the difference in the formation or how to stuff between
baking soda and Naoh??????? Thanks? A010
|
cactus Member |
posted 11-09-1999 03:52 PM
Bennie Yes you place the toulene solution that was setting on top of the
reation solution into a bowl.
Before the solution is poured into bowl the toulene that was setting on
top of the solution had a small amount of lye sprinkled on top. The lye
will go to the bottom and streams of bubbles will surface.
When you place the top layer into the bowl by pulling with a sqeeze
bottle. It then is gassed to see if crystals are produced. If it doesnt
add acitone and whatch for a minute if nothing happens then place the bowl
into the microwave for 3 or 4 minutes depending on how much solvent is
there. I believe this removes water and reduces the solvent. Take out the
bowl and place under a fan and the material will start producing
cyristals.
This has to be done in a dry atmosphere such as modern air condition.
You can place the bowl in front of your return vent of your central air
handler.
Then just add another batch of toulene on top of the reaction fluid and
repeat obove step.
Any time you pull off the reaction water filter the toulene. Also the
Sodium Hydroxide sticks to glass so just keep tranfering to other clean
glass containers untill lye isn't sticking to glass.
I wipe the glass off with blue paper shop towels.
------------------ Live With Freedom
|
FMAN Member |
posted 11-09-1999 04:30 PM
Wor 10-30 the problemo could be related to hydrogen donator in the water
part of the solution, now I aint shure wich solvent is being employed
exactly, but the multi thing and freeze works good for most, considering
the possiblity of the hydrogen sucking off the fuel layer and falling into
a trap in the water layer is a definate possibility, allowing the hydrogen
in the solvent to stabalize might be necessary to remove the water portion
of the solvent in classic situation, thus is the thing being done in the
Dron style or is it being done in classic style? In a test tube the
freebased stuff in solvent is washed with a lye solution to alow some
water soluable contaminates out, hopefully this is a heavy water compared
to the solvent? Then the lye is further washed out with a portion of pure
water, leaving a better solution to work with in theory, how rushed this
becomes can be an important consideration, thus poor guy is in a hurry? Um
so a drop of indicator is added with a drop of water into the test tube
containing the suspect salt to issolate and it is adjusted to the proper
PH evident by shaking and allowing resolution of the water droplets on the
bottom layer, the color in this droplet changes as acid is added, this is
the indicator Hum so ya can add
some acid to some base and ya form salt, good very well understand how to
make salt and how to undo salt. Hum so this is the real question? No, guy
complains of a bunch of gak, um poision? Hummm well One might try to
issolate from the mixture the salt and the amine, now considering if ya
gots salt and amine in solution the solution is then allowed to resolve
without heat into crytstals, these crystals might be salt or amine salt
crystals??? Well at this specific issoellectric point not discussed it
aint the question,,,anyways the amine salt will also ussually occur
unless......oh if the salt HCL is in compound resembling our target
molecule it is not preferentually reduced or otherwise gasses off the
solution in preference or before simple stuff that in the like of this
idea means salt.....we know ammonia loves water and also salt but under
certain circumstances the salt does not love water as much as the ammonia,
who has frozen water to seperate ammonia? anyways the salt will stay in
the water wheras the uncomplicated salt will leave, thus lye is removed
from and influenced by gravity, and at othertimes becomes boyant, dont
ask. Anyways the por thing has allready been displayed and a ground or
nutral pH has allready been reported, how to adjust this to macroscal will
involve allowing the somic stuff in there or the poor thing is gona need
some awfull violent and complex lasser stuff, to also likewise initiate
the appropiate cascade of events, needless to say this is a hurry thing?
Gosh be boggle ya might have something in there that has not been
isolated,,,ok so try different method, make super chilled of that stuff
the solvent and make shure it has whtever gak might be dumped in there all
kinda stuff, make a good and diversive mixture of solvent stuff and grind
the goodies up, how to get rid of or deactivate the phosphor seems to be a
little problem but who knows I can easilly deactivate a cn, so if there is
a good way um I aint seen it...Maybe I just dont know how to get rid of
the phosphor question without having titled or been real specific it seems
like more of and end to itself at this juncture is a waste of my time. I
would add some wtare and have available some acid in that water at the
same token I would employ a multi role to all solution and chemical
mixtures immediatly and if issolating a specific regemin keep it simple
like NA this is not a comercial venture,,,the best way to rid the phosphor
question seems paramount as a critism in my opinion herin the report is a
complaint about the process, why do I dont get the real reason to add
phosphorus straight into the reaction mixture it just aint propper
|
FMAN Member |
posted 11-09-1999 05:22 PM
You are making salt water to preferientiate the leaving of the basic amine
[partner acid is attached] to the solvent layer wich is high in trapped
hydrogen content, see adding lye does make salt and it steals this salt
stuff from the lesser ammine to make ions in the water[which is less basic
than the amine?],oh the water becomes more basic than the amine of courrse
the ammine
is then allowed to seek a more compatable and stable friend in the solvent
which for pracality is said to be saturated in hydrogen. Thus the amine
tries to move into solvent at potential of concerning the issoellectric
point, adjusting it to the said PH um is a little extravigant, in nay case
causes the thing to go into the solvent ussually never the less, the key
point here is that the stronger base formed in water solution and thus the
amine is repelled out of or forced to the edges, and in glass if ya
overpotentiate the lye the lye attacks the glass, anyways the whole might
be corrected buy employing a gradual tempature gradient against the
solution containg the water, thus at PH of say 7+ in the water and the
stuff in there the lye it is or becomes supersaturate at a point of say X
pressure and water is a cooler pressure thing thatn anything else I know
of, so if we reduce the tempature less salt or lye in this case is allowed
to reside in the solution and or does the PH change? Well it is a very
good question??? Hum so um a I am still investigationg this phenomena,
seemingly allthough the pH has not changed this does become a very
different method alltogether, so as ya cool this salt water something real
weird happens the lye and salt formed becomes reentrained in the water
matrix, and most of the impurity is forced out the impurity happens to be
the stuff we want anyways, and little gas bubbles of water appear in the
forming solid water mass as the result of? Um maybe the latice is reacting
to um it is allowing the salt to become seperate than it forming little
cages of gas or emptyness around dirt or salt, and these empty cages might
be in time discovered to contain say the complimentary netralization gass
found in the water to nutralize the um contaminant, this in this case
being Hydrogen for clorine and oxygen for sodium and sometimes other trace
gasses are employed as the result it is indeed a very complex rational to
evolve into hering this is the basic rational for it, understand or fail.
Many gasses are present in water such as in to certain degree to whatever
catalyst might be contained therin, thus co might be at a very high level
in pure water before alowing for expulsion wherass oxygen gas is at a
minumium....hummmm so argon and nitrogen are also in there, of course
these can all be measure with appropiate equipment which is much more
complex than suited for clandestine discussion presently, clandestine may
mean you dont know why but it happens because it is the way it is and ya
cant change this So considering
the ammine has left the water to allow it into a hydrogen attractant in
the solvent,, humm adding the above paradigm is allowed in reverse from
the classic water thing, see if solvent or oil is allowed to float or
become light, in this case it aint soluable inwater due to it has become
light in any case and has disolved into the solvent due to the attration
of the hydrogen component in the lkattice there, along the way it will be
discovered also that some strange stuff is in the solvent and that will be
gass of metal or rather more appropiate could be considered a carbon
coponent or cyanide might be in there which also attarcts finly divided
metals in well in my investigations this acts equall to the watereffect
which works good for myself in any case....ok so as the water cools it is
further complicated by the gasses in the solvent and seemingly a membrane
potential or gas difussion complicating and mitigating factor is present,
thus it aint water and we know ammonia compounds usually love water but in
this case most all of the water is getting sucked out as gas into the
water becoming solid as to solvate the supersaturated condition it is
becomming, I wa allway mystified by those strange stalagmite forms
erupting from the ice surface, aside from that it does eventually seem to
reform and resolve but a groth factor has to be considered? What has
happened to cause the ammine to seperate from the solvent well we know
that the gass above the vessel is constant and a vacume is being created
and also this vacume is alowed to pass through the solvent and pressure is
alluted in the ice, the hydrogen gas is suched into the crystaline latice
preferentually because it is solvent, and solvent does love hydrogen
stuff, and amine still loves the water but is attracted to the solvent,
considering pressure and tempature are as constant and related to
eachother as proposed and vacume is flowing through the solvent into the
water which is becoming solidified and in ever constant need of more gass
to nutralize itself, well it the amine is allowed to seperate out into the
middle, um ya cant see it, hum bummer, ok so ya add something for the
ammine to be attracted to um like likes like, so considering this thing
likes is alot like something that can be moved into position to attract
the ammine and also alow crystalization, this can be a complex issue,
considering all that salt in the water layer, I just cant think of a way
to employ such a salt for the extraction of such a similiar thing such as
our product. Thus ya need to extract the dam salt of away from the product
before hand to make it um work. although it might work anyways and in all
kinda solvent and conditions with or without mitigating factors, the main
problemo of the future will be issolating and seperating complex salts
that are very similiar in all behavior to the target salts, because there
are some deranged individuals who consider profit a supreem virtue and
they will not alow shortcuts from there dividend. Um starting from raw
product even if messed with with minimal effort the amine will allways be
a easy thing to issolate I am shure of this fact, and that plants may be
rown or fertalized in a away to capatalize on complex formation of various
salts that could be or need not be purified in any manner, although the
technology exists it will allways be the natual and basic thigns that pull
ya through the more of these ya master will result in further
clarification and differentiation from total bullish from stuff that is
praticall for you at any given point in time hopefully less and less
things sem bullish and ya try them in reality, it is my sinceere hop to
find you crystal grown in a container near you if you so desire one -A010
|